 |
Radiochemical Analysis
|
PARAMETER
|
METHOD
|
METHOD
DESCRIPTION
|
MATRIX
|
VOLUME
REQUIRED
|
CONTAINER
|
PRESERVATIVE
|
|
|
Americium 241
|
EPA 907(M)
or
DOE EML HASL 300 4.5.4 (M)
|
Alpha Spectroscopy
or
Gamma Spectrometry
|
W
WW
S
SW
F
|
1000 ml
1000 ml
500 g
500 g
NA
|
P,G
P,G
P,G
P,G
P,G
|
HNO3 to pH< 2
HNO3 to pH< 2
NA
NA
NA
|
|
|
Carbon -14
|
USEPA (EPA-P4-73-014) C-14
|
Liquid Scintillation
|
W
WW
S
SW
F
|
1000 ml
1000 ml
500 g
500 g
NA
|
P,G
P,G
P,G
P,G
P,G
|
Cool < 4oC
Cool < 4oC
Cool < 4oC
Cool < 4oC
NA
|
|
|
Gamma Spectrometry
Please Refer to Gamma Table for Isotopes
|
EPA 901.1
or
DOE EML HASL 300 4.5.4 (M)
|
Gamma Spectroscopy
|
W
WW
S
SW
F
|
1000 ml
1000 ml
500 g
500 g
NA
|
P,G
P,G
P,G
P,G
P,G
|
HNO3 to pH< 2
HNO3 to pH< 2
NA
NA
NA
|
|
|
Gross Alpha/Beta
|
EPA 900
SW9310
|
Gas Proportional Counting
|
W
WW
S
SW
F
|
500 ml
500 ml
10 g
10 g
NA
|
P,G
P,G
P,G
P,G
P,G
|
HNO3 to pH< 2
HNO3 to pH< 2
NA
NA
NA
|
|
|
Iodine-129
|
EPA 901.1
or
DOE EML HASL 300 4.5.4 (M)
|
X-Ray Spectroscopy
|
W
WW
S
SW
F
|
1000 ml
1000 ml
500 g
500 g
NA
|
P,G
P,G
P,G
P,G
P,G
|
NA
NA
NA
NA
NA
|
|
|
Iron 55
|
ASTM D4922
|
Liquid Scintillation
|
W
WW
S
SW
F
|
1000 ml
1000 ml
10 g
10 g
NA
|
P,G
P,G
P,G
P,G
P,G
|
HNO3 to pH< 2
HNO3 to pH< 2
NA
NA
NA
|
|
|
Lead 210
|
|
Gas Proportional Counting
Or
Gamma Spectroscopy
|
W
WW
S
SW
F
|
1000 ml
1000ml
500 g
500 g
NA
|
P,G
P,G
P,G
P,G
P,G
|
HNO3 to pH< 2
HNO3 to pH< 2
NA
NA
NA
|
|
PARAMETER
|
METHOD
|
METHOD
DESCRIPTION
|
MATRIX
|
VOLUME
REQUIRED
|
CONTAINER
|
PRESERVATIVE
|
|
|
Neptunium 237
|
EPA 907(M) or
DOE EML HASL 300 4.5.4 (M)
|
Alpha Spectroscopy
or
Gamma Spectrometry
|
W
WW
S
SW
F
|
1000 ml
1000 ml
500 g
500 g
NA
|
P,G
P,G
P,G
P,G
P,G
|
HNO3 to pH< 2
HNO3 to pH< 2
NA
NA
NA
|
|
|
Nickel 59, 63
|
RESL CHEM-TP-Ni.1
|
Liquid Scintillation
|
W
WW
S
SW
F
|
1000 ml
1000 ml
10 g
10 g
NA
|
P,G
P,G
P,G
P,G
P,G
|
HNO3 to pH< 2
HNO3 to pH< 2
NA
NA
NA
|
|
|
Polonium 210
|
DOE EML HASL 300
Po-02 (M)
|
Alpha Spectroscopy
|
W
WW
S
SW
F
|
1000 ml
1000 ml
10 g
10 g
NA
|
P,G
P,G
P,G
P,G
P,G
|
HNO3 to pH< 2
HNO3 to pH< 2
NA
NA
NA
|
|
|
Plutonium (Isotopic)
238, 239/240
|
EPA 907(M)
Or
LANL ER160
|
Alpha Spectroscopy
|
W
WW
S
SW
F
|
1000 ml
1000 ml
10 g
10 g
NA
|
P,G
P,G
P,G
P,G
P,G
|
HNO3 to pH< 2
HNO3 to pH< 2
NA
NA
NA
|
|
|
Radium, Total Alpha
|
SM7500Ra
|
Gas Proportional Counting
|
W
WW
S
SW
F
|
1000 ml
1000 ml
10 g
10 g
NA
|
P,G
P,G
P,G
P,G
P,G
|
HNO3 to pH< 2
HNO3 to pH< 2
NA
NA
NA
|
|
|
Radium 223
|
SM7500Ra (M)
or
DOE EML HASL 300 4.5.4 (M)
|
Alpha Spectroscopy
or
Gamma Spectrometry
|
W
WW
S
SW
F
|
1000 ml
1000 ml
500 g
500 g
NA
|
P,G
P,G
P,G
P,G
P,G
|
HNO3 to pH< 2
HNO3 to pH< 2
NA
NA
NA
|
|
|
Radium 224
|
SM7500Ra (M)
or
DOE EML HASL 300 4.5.4 (M)
|
Alpha Spectroscopy
or
Gamma Spectrometry
|
W
WW
S
SW
F
|
1000 ml
1000 ml
500 g
500 g
NA
|
P,G
P,G
P,G
P,G
P,G
|
HNO3 to pH< 2
HNO3 to pH< 2
NA
NA
NA
|
|
PARAMETER
|
METHOD
|
METHOD
DESCRIPTION
|
MATRIX
|
VOLUME
REQUIRED
|
CONTAINER
|
PRESERVATIVE
|
|
|
Radium 226
|
SM7500Ra (M)
or
DOE EML HASL 300 4.5.4 (M)
|
Alpha Spectroscopy
or
Gamma Spectrometry
|
W
WW
S
SW
F
|
1000 ml
1000 ml
500 g
500 g
NA
|
P,G
P,G
P,G
P,G
P,G
|
HNO3 to pH< 2
HNO3 to pH< 2
NA
NA
NA
|
|
|
Radium 228
|
EPA 904/SW9320
or
DOE EML HASL 300 4.5.4 (M)
|
Gas Proportional Counting
or
Gamma Spectrometry
|
W
WW
S
SW
F
|
1000 ml
1000 ml
500 g
500 g
NA
|
P,G
P,G
P,G
P,G
P,G
|
HNO3 to pH< 2
HNO3 to pH< 2
NA
NA
NA
|
|
|
Radon 222
|
SM 7500Rn
|
Liquid Scintillation
|
W
WW
F
|
1000 ml
1000 ml
NA
|
P,G
P,G
P,G
|
Cool < 4oC
Cool < 4oC
NA
|
|
|
Strontium 89
|
EPA 905
|
Gas Proportional Counting
|
W
WW
S
SW
F
|
1000 ml
1000 ml
10 g
10 g
NA
|
P,G
P,G
P,G
P,G
P,G
|
HNO3 to pH< 2
HNO3 to pH< 2
NA
NA
NA
|
|
|
Strontium 90
|
EPA 905
|
Gas Proportional Counting
|
W
WW
S
SW
F
|
1000 ml
1000 ml
10 g
10 g
NA
|
P,G
P,G
P,G
P,G
P,G
|
HNO3 to pH< 2
HNO3 to pH< 2
NA
NA
NA
|
|
|
Technetium 99
|
ESSAP Section 14
or
DOE EML HASL 300
(TC-01-RC)
|
Gas Proportional Counting or Liquid Scintillation
|
W
WW
S
SW
F
|
1000 ml
1000 ml
10 g
10 g
NA
|
G
G
G
G
G
|
HNO3 to pH< 2
HNO3 to pH< 2
NA
NA
NA
|
|
|
Thorium (Isotopic)
228,230, 232
|
DOE LANL ER200
|
Alpha Spectroscopy
|
W
WW
S
SW
F
|
1000 ml
1000 ml
10 g
10 g
NA
|
P,G
P,G
P,G
P,G
P,G
|
HNO3 to pH< 2
HNO3 to pH< 2
NA
NA
NA
|
|
PARAMETER
|
METHOD
|
METHOD
DESCRIPTION
|
MATRIX
|
VOLUME
REQUIRED
|
CONTAINER
|
PRESERVATIVE
|
|
|
Tritium (H3)
|
EPA 906
|
Liquid Scintillation
|
W
WW
S
SW
F
|
1000 ml
1000 ml
10 g
10 g
NA
|
G
G
G
G
G
|
NA
NA
NA
NA
NA
|
|
|
Uranium (Isotopic)
234, 235,238
|
ASTM D3972
|
Alpha Spectroscopy
|
W
WW
S
SW
F
|
1000 ml
1000 ml
10 g
10 g
NA
|
P,G
P,G
P,G
P,G
P,G
|
HNO3 to pH< 2
HNO3 to pH< 2
NA
NA
NA
|
|
|
Uranium Total
|
ASTM D5174
|
Laser Kinetic Phosphorimetry
|
W
WW
S
SW
F
|
20 ml
20 ml
10 g
10 g
NA
|
P,G
P,G
P,G
P,G
P,G
|
HNO3 to pH< 2
HNO3 to pH< 2
NA
NA
NA
|
|
GAMMA SPECTRSCOPY
|
NORM
|
Gamma Spectroscopy*
|
|
Actinium 228(Ra228 and Th232)
Bismuth 212
Bismuth 214(Ra226)
Lead 212
Lead 214(Ra226)
Potassium 40
Thallium 204
Thorium 234 (Uranium 238)
|
Americium 241
Barium 133
Cesium 134
Cesium 137
Cobalt 57
Cobalt 60
Europium 152
Europium 154
Europium 155
Iodine 129
Iodine 131
Iridium 192
Manganese 54
Mercury 203
Neodymium 147
Niobium 94
Niobium 95
Yttrium 88
Zinc 65
Zirconium 95
|
* Please call if additional isotopes are required.
|
|
|
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