 |
Organic Analysis
|
GC/MS ANALYSIS
Metals can be analysed individually or as a group.
PARAMETER
|
METHOD
|
METHOD
DESCRIPTION
|
MATRIX
|
VOLUME
REQUIRED
|
CONTAINER
|
PRESERVATIVE
|
|
|
Volatile Compounds
|
SW 846 8260B
Or
EPA 624
|
Gas Chromatography/Mass Spectrometry
|
W
WW
S
SW
TCLP
|
3x40 ml
3x40 ml
4oz
4oz
8oz
|
G*
G*
G*
G*
G*
|
Cool < 4oC
Cool < 4oC
Cool < 4oC
Cool < 4oC
Cool < 4oC
|
|
*40 ml zero headspace vial required
GC/MS ANALYSIS
Metals can be analysed individually or as a group.
PARAMETER
|
METHOD
|
METHOD
DESCRIPTION
|
MATRIX
|
VOLUME
REQUIRED
|
CONTAINER
|
PRESERVATIVE
|
|
|
Semi-Volatile Compounds
|
SW 846 8270C
Or
EPA 625
|
Gas Chromatography/Mass Spectrometry
|
W
WW
S
SW
TCLP
|
2x1000 ml
2x1000 ml
8oz
8oz
16oz
|
(Amber)G
(Amber)G
G
G
G
|
Cool < 4oC
Cool < 4oC
Cool < 4oC
Cool < 4oC
Cool < 4oC
|
|
GC ANALYSIS
PARAMETER
|
METHOD
|
METHOD
DESCRIPTION
|
MATRIX
|
VOLUME
REQUIRED
|
CONTAINER
|
PRESERVATIVE
|
|
|
Herbicides
|
SW 846 8151
|
Gas Chromatograph/ECD
|
W
WW
S
SW
TCLP
|
2x1000 ml
2x1000 ml
8oz
8oz
16oz
|
(Amber)G
(Amber)G
G
G
G
|
Cool < 4oC
Cool < 4oC
Cool < 4oC
Cool < 4oC
Cool < 4oC
|
|
GC ANALYSIS
PARAMETER
|
METHOD
|
METHOD
DESCRIPTION
|
MATRIX
|
VOLUME
REQUIRED
|
CONTAINER
|
PRESERVATIVE
|
|
|
PCB’s
|
SW 846 8082
Or
EPA 608
|
Gas Chromatograph/ECD
|
W
WW
S
SW
TCLP
Oil
|
2x1000 ml
2x1000 ml
8oz
8oz
16oz
25 ml
|
(Amber)G
(Amber)G
G
G
G
G,P
|
Cool < 4oC
Cool < 4oC
Cool < 4oC
Cool < 4oC
Cool < 4oC
Cool < 4oC
|
|
|
Pesticides
|
SW 846 8081
Or
EPA 608
|
Gas Chromatograph/ECD
|
W
WW
S
SW
TCLP
|
2x1000 ml
2x1000 ml
8oz
8oz
16oz
|
(Amber)G
(Amber)G
G
G
G
|
Cool < 4oC
Cool < 4oC
Cool < 4oC
Cool < 4oC
Cool < 4oC
|
|
|
Total Petroleum Hydrocarbons
(Diesel Range)
|
SW 846 8015B(M)
|
Gas Chromatograph/FID
|
W
WW
S
SW
TCLP
|
2x1000 ml
2x1000 ml
8oz
8oz
16oz
|
(Amber)G
(Amber)G
G
G
G
|
Cool < 4oC
Cool < 4oC
Cool < 4oC
Cool < 4oC
Cool < 4oC
|
|
|
Total Petroleum Hydrocarbons
(Gasoline Range)
|
SW 846 8015B(M)
|
Gas Chromatograph/FID
|
W
WW
S
SW
TCLP
|
3x40 ml
3x40 ml
4oz
4oz
8oz
|
G*
G*
G
G
G
|
Cool < 4oC
Cool < 4oC
Cool < 4oC
Cool < 4oC
Cool < 4oC
|
|
*40 ml zero headspace vial required
Volatile Organic Compounds
|
SW 846 8260
|
|
Dichlorodifluoromethane
Chloromethane
Vinyl chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
Diethyl ether
Acetone
1,1-Dichloroethene
Methylene chloride
trans-1,2-Dichloroethene
1,1-Dichloroethane
2-Butanone (MEK)
2,2-Dichloropropane
cis-1,2-Dichloroethene
Ethyl acetate
Chloroform
Bromochloromethane
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon tetrachloride
1,2-Dichloroethane
Benzene
2-Pentanone
Trichloroethene
1,2-Dichloropropane
Bromodichloromethane
Dibromomethane
|
4-Methyl-2-pentanone (MIBK)
4-Isopropyltoluene
cis-1,3-Dichloropropene
1,3-Dichlorobenzene
Toluene
1,4-Dichlorobenzene
trans-1,3-Dichloropropene
n-Butylbenzene
1,1,2-Trichloroethane
1,2-Dichlorobenzene
2-Hexanone
1,2-Dibromo-3-chloropropane
1,3-Dichloropropane
1,2,4-Trichlorobenzene
Tetrachloroethene
Hexachlorobutadiene
Dibromochloromethane
Naphthalene
1,2-Dibromoethane (EDB)
1,2,3-Trichlorobenzene
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
p&m-Xylene
o-Xylene
Styrene
Bromoform
Isopropylbenzene
|
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
n-Propylbenzene
Bromobenzene
1,3,5-Trimethylbenzene
2-Chlorotoluene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
|
Volatile Organic Compounds
|
Priority Pollutants
|
|
Dichlorodifluoromethane
Vinyl chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene chloride
trans-1,2-Dichloroethene
1,1-Dichloroethane
Chloroform
2-chloroethylvinyl ether
1,1,1-Trichloroethane
Carbon tetrachloride
1,2-Dichloroethane
Benzene
|
cis-1,3-Dichloropropene
Toluene
trans-1,3-Dichloropropene
1,1,2-Trichloroethane
Tetrachloroethene
Dibromochloromethane
Chlorobenzene
Ethylbenzene
Bromoform
1,1,2,2-Tetrachloroethane
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,2-Dichlorobenzene
Methyl Bromide
Methyl Chloride
|
Acrolein
Acryonitrile
Trichloroethene
1,2-Dichloropropane
Bromodichloromethane
|
|
TTO
|
|
Vinyl chloride
Chloroethane
1,1-Dichloroethene
Methylene chloride
trans-1,2-Dichloroethene
1,1-Dichloroethane
Chloroform
2-chloroethylvinyl ether
1,1,1-Trichloroethane
Carbon tetrachloride
1,2-Dichloroethane
Benzene
|
cis-1,3-Dichloropropene
Toluene
trans-1,3-Dichloropropene
1,1,2-Trichloroethane
Tetrachloroethene
Dibromochloromethane
Chlorobenzene
Ethylbenzene
Bromoform
1,1,2,2-Tetrachloroethane
Methyl Bromide
Methyl Chloride
|
Acrolein
Acryonitrile
Trichloroethene
1,2-Dichloropropane
Bromodichloromethane
|
Volatile Organic Compounds
|
Target Compound List (TCL)
|
|
Vinyl acetate
Vinyl chloride
Acetone
Chloroethane
Carbon disulfide
1,1-Dichloroethene
Methylene chloride
2-Butanone (MEK)
1,1-Dichloroethane
Chloroform
2-Hexanone
1,1,1-Trichloroethane
Carbon tetrachloride
1,2-Dichloroethane
Benzene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
Trichloroethene
1,2-Dichloropropane
Bromodichloromethane
|
cis-1,3-Dichloropropene
Toluene
trans-1,3-Dichloropropene
1,1,2-Trichloroethane
Tetrachloroethene
Dibromochloromethane
Chlorobenzene
Ethylbenzene
Bromoform
1,1,2,2-Tetrachloroethane
Styrene
4-Methyl-2-pentanone (MIBK)
Xylenes (Total)
Methyl Bromide
Methyl Chloride
|
|
|
Toxic Chemical Leaching Procedure (TCLP)
|
|
Vinyl chloride
1,1-Dichloroethene
2-Butanone (MEK)
Chloroform
Carbon tetrachloride
1,2-Dichloroethane
Benzene
Trichloroethene
|
Tetrachloroethene
Chlorobenzene
1,4-Dichlorobenzene
|
|
Semi-Volatile Organic Compounds
|
8270C
|
|
N-nitrosodimethylamine
Pyridine
Phenol
bis (2-Chloroethyl) ether
2-Chlorophenol
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,2-Dichlorobenzene
2-Methylphenol
4-Methylphenol
n-Nitroso-di-n-propylamine
Hexachloroethane
Nitrobenzene
Isophorone
2-Nitrophenol
2,4-Dimethylphenol
Benzoic Acid
bis (2-chloroethoxy) methane
2,4-Dichlorophenol
1,2,4-Trichlorobenzene
Naphthalene
4-Chloroaniline
Hexachlorobutadiene
4-Chloro-3-methylphenol
|
2-Methylnaphthalene
Hexachlorocyclopentadiene
2,4,6-Trichlorophenol
2,4,5-Trichlorophenol
2-Chloronaphthalene
2-Nitroaniline
Dimethylphathalate
Acenaphthylene
3-Nitroaniline
Acenaphthene
2,4-Dinitrophenol
4-Nitrophenol
Dibenzofuran
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Diethylphthalate
4-Chlorophenyl phenyl ether
Fluorene
4-Nitroaniline
4,6-Dinitro-2-methylphenol
4-Bromophenyl phenyl ether
Hexachlorobenzene
Pentachlorophenol
Phenanthrene
|
Anthracene
Carbazole
Di-n-butylphthalate
Fluoranthene
Benzidine
Pyrene
Butylbenzylphthalate
3,3'-Dichlorobenzidine
Benzo (a) anthracene
bis (2-Ethylhexyl) phthalate
Chrysene
Di-n-octyl phthalate
Benzo (b) fluoranthene
Benzo (k) fluroanthene
Benzo (a) pyrene
Indeno (1,2,3-cd) pyrene
Dibenz(a,h) anthracene
Benzo (g,h,i) perylene
Azobenzene
bis (2-chloroisopropyl) ether
|
Semi-Volatile Organic Compounds
|
Priority Pollutants
|
|
N-nitrosodimethylamine
Phenol
bis (2-Chloroethyl) ether
2-Chlorophenol
Hexachloroethane
Nitrobenzene
Isophorone
2-Nitrophenol
2,4-Dimethylphenol
bis (2-chloroethoxy) methane
2,4-Dichlorophenol
1,2,4-Trichlorobenzene
Naphthalene
Hexachlorobutadiene
4-Chloro-3-methylphenol
1,2-Diphenylhydrazine
|
Hexachlorocyclopentadiene
2,4,6-Trichlorophenol
2-Chloronaphthalene
Dimethylphathalate
Acenaphthylene
Acenaphthene
2,4-Dinitrophenol
4-Nitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Diethylphthalate
4-Chlorophenyl phenyl ether
Fluorene
4,6-Dinitro-2-methylphenol
4-Bromophenyl phenyl ether
Hexachlorobenzene
Pentachlorophenol
Phenanthrene
|
Anthracene
Di-n-butylphthalate
Fluoranthene
Benzidine
Pyrene
Butylbenzylphthalate
3,3'-Dichlorobenzidine
Benzo (a) anthracene
bis (2-Ethylhexyl) phthalate
Chrysene
Di-n-octyl phthalate
Benzo (b) fluoranthene
Benzo (k) fluroanthene
Benzo (a) pyrene
Indeno (1,2,3-cd) pyrene
Dibenz(a,h) anthracene
Benzo (g,h,i) perylene
bis (2-chloroisopropyl) ether
|
|
TTO
|
|
Phenol
bis (2-Chloroethyl) ether
2-Chlorophenol
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,2-Dichlorobenzene
n-Nitroso-di-n-propylamine
Hexachloroethane
Nitrobenzene
Isophorone
2-Nitrophenol
2,4-Dimethylphenol
bis (2-chloroethoxy) methane
2,4-Dichlorophenol
1,2,4-Trichlorobenzene
Naphthalene
Hexachlorobutadiene
4-Chloro-3-methylphenol
1,2-Diphenylhydrazine
|
Hexachlorocyclopentadiene
2,4,6-Trichlorophenol
2-Chloronaphthalene
Dimethylphathalate
Acenaphthylene
Acenaphthene
2,4-Dinitrophenol
4-Nitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Diethylphthalate
4-Chlorophenyl phenyl ether
Fluorene
4,6-Dinitro-2-methylphenol
4-Bromophenyl phenyl ether
Hexachlorobenzene
Pentachlorophenol
Phenanthrene
Diphenylamine
|
Anthracene
Di-n-butylphthalate
Fluoranthene
Benzidine
Pyrene
Butylbenzylphthalate
3,3'-Dichlorobenzidine
Benzo (a) anthracene
bis (2-Ethylhexyl) phthalate
Chrysene
Di-n-octyl phthalate
Benzo (b) fluoranthene
Benzo (k) fluroanthene
Benzo (a) pyrene
Indeno (1,2,3-cd) pyrene
Dibenz(a,h) anthracene
Benzo (g,h,i) perylene
bis (2-chloroisopropyl) ether
|
Semi-Volatile Organic Compounds
|
Target Compound List (TCL)
|
|
Phenol
bis (2-Chloroethyl) ether
2-Chlorophenol
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,2-Dichlorobenzene
2-Methylphenol
3,4-Methylphenol
n-Nitroso-di-n-propylamine
Hexachloroethane
Nitrobenzene
Isophorone
2-Nitrophenol
2,4-Dimethylphenol
bis (2-chloroethoxy) methane
2,4-Dichlorophenol
1,2,4-Trichlorobenzene
Naphthalene
4-Chloroaniline
Hexachlorobutadiene
4-Chloro-3-methylphenol
1,1’-Biphenyl
Acetophenone
Atrazine
|
2-Methylnaphthalene
Hexachlorocyclopentadiene
2,4,6-Trichlorophenol
2,4,5-Trichlorophenol
2-Chloronaphthalene
2-Nitroaniline
Dimethylphathalate
Acenaphthylene
3-Nitroaniline
Acenaphthene
2,4-Dinitrophenol
4-Nitrophenol
Dibenzofuran
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Diethylphthalate
4-Chlorophenyl phenyl ether
Fluorene
4-Nitroaniline
4,6-Dinitro-2-methylphenol
4-Bromophenyl phenyl ether
Hexachlorobenzene
Pentachlorophenol
Phenanthrene
|
Anthracene
Carbazole
Di-n-butylphthalate
Fluoranthene
Benzidine
Pyrene
Butylbenzylphthalate
3,3'-Dichlorobenzidine
Benzo (a) anthracene
bis (2-Ethylhexyl) phthalate
Chrysene
Di-n-octyl phthalate
Benzo (b) fluoranthene
Benzo (k) fluroanthene
Benzo (a) pyrene
Indeno (1,2,3-cd) pyrene
Dibenz(a,h) anthracene
Benzo (g,h,i) perylene
bis (2-chloroisopropyl) ether
Benzaldehyde
Caprolactam
Diphenylamine
|
|
Toxic Chemical Leaching Procedure (TCLP)
|
|
Pyridine
1,4-Dichlorobenzene
2-Methylphenol
3,4-Methylphenol
Hexachloroethane
Nitrobenzene
Hexachlorobutadiene
|
2,4,6-Trichlorophenol
2,4,5-Trichlorophenol
2,4-Dinitrotoluene
Hexachlorobenzene
Pentachlorophenol
|
|
Pesticide/PCB/Herbicide Compounds
|
Pesticides SW 846 8081
|
PCB’s SW846 8082
|
Herbicides SW 846 8151
|
|
Alpha-BHC
Beta-BHC
Delta-BHC
Gamma BHC (Lindane)
Chlordane
Alpha-Chlordane
Gamma-Chlordane
4,4’-DDD
4,4’-DDE
4,4’ DDT
Dieldrin
Endosulfan I
Endosulfan II
Endosulfan Sulfate
Endrin
Endrin Aldehyde
Endrin Ketone
Heptachlor
Heptachlor Epoxide
Methoxychlor
Toxaphene
|
PCB-1221
PCB-1232
PCB-1242
PCB-1248
PCB-1254
PCB-1260
|
|
|
Pesticides Priority Pollutants
|
PCB’s Priority Pollutants
|
Herbicides Priority Pollutants
|
|
Alpha-BHC
Beta-BHC
Delta-BHC
Gamma BHC (Lindane)
4,4’-DDD
4,4’-DDE
4,4’ DDT
Dieldrin
Endosulfan I
Endosulfan II
Endosulfan Sulfate
Endrin
Endrin Aldehyde
Heptachlor
Heptachlor Epoxide
Methoxychlor
Toxaphene
|
PCB-1221
PCB-1232
PCB-1242
PCB-1248
PCB-1254
PCB-1260
|
|
|
|
|
|
Pesticide/PCB/Herbicide Compounds
|
Pesticides Target Compound List (TCL)
|
PCB’s Target Compound List (TCL)
|
Herbicides Target Compound List (TCL)
|
|
Alpha-BHC
Beta-BHC
Delta-BHC
Gamma BHC (Lindane)
Alpha-Chlordane
Gamma-Chlordane
4,4’-DDD
4,4’-DDE
4,4’ DDT
Dieldrin
Endosulfan I
Endosulfan II
Endosulfan Sulfate
Endrin
Endrin Ketone
Heptachlor
Heptachlor Epoxide
Methoxychlor
Toxaphene
|
PCB-1221
PCB-1232
PCB-1242
PCB-1248
PCB-1254
PCB-1260
|
|
|
Pesticides TCLP
|
PCB’s TCLP
|
Herbicides TCLP
|
|
Gamma BHC (Lindane)
Endrin
Heptachlor
Heptachlor Epoxide
Methoxychlor
Toxaphene
Chlordane
|
|
2,4,5-TP (Silvex)
|
|
Pesticides TTO
|
PCB’s TTO
|
|
Alpha-BHC
Beta-BHC
Delta-BHC
Gamma BHC (Lindane)
4,4’-DDD
4,4’-DDE
4,4’ DDT
Dieldrin
|
Endosulfan I
Endosulfan II
Endosulfan Sulfate
Endrin
Endrin Aldehyde
Heptachlor
Heptachlor Epoxide
|
PCB-1221
PCB-1232
PCB-1242
PCB-1248
PCB-1254
PCB-1260
|
|
|
|
|
|
|
|
|
|
 |
 |
|
|
