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Organic Analysis
PARAMETER |
METHOD |
METHOD |
MATRIX |
VOLUME REQUIRED |
CONTAINER |
PRESERVATIVE |
HOLDING |
|
Volatile Compounds |
SW846
8260B OR EPA 624 |
Gas Chromatography/Mass Spectrometry |
W |
3x40 ml |
G* |
Cool < 4oC |
14 days |
| WW | 3x40 ml | G* | Cool < 4oC | 14 days | |||
| S | 4oz | G* | Cool < 4oC | 14 days | |||
| SW | 4oz | G* | Cool < 4oC | 14 days | |||
| TCLP | 8oz | G* | Cool < 4oC | 14 days |
|
*40 ml zero headspace vial required
|
PARAMETER |
METHOD |
METHOD |
MATRIX |
VOLUME REQUIRED |
CONTAINER |
PRESERVATIVE |
HOLDING |
|
Semi-Volatile Compounds |
SW846
8270C OR EPA 625 |
Gas Chromatography/Mass Spectrometry |
W |
2x1000 ml |
(Amber)G |
Cool < 4oC |
14 days |
| WW | 2x1000 ml | (Amber)G | Cool < 4oC | 14 days | |||
| S | 8oz | G | Cool < 4oC | 14 days | |||
| SW | 8oz | G | Cool < 4oC | 14 days | |||
| TCLP | 16oz | G | Cool < 4oC | 14 days |
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GC ANALYSIS |
PARAMETER |
METHOD |
METHOD |
MATRIX |
VOLUME REQUIRED |
CONTAINER |
PRESERVATIVE |
HOLDING |
|
Herbicides |
SW846
8151 |
Gas Chromatograph/ECD |
W |
2x1000 ml |
(Amber)G |
Cool < 4oC |
7 days |
| WW | 2x1000 ml | (Amber)G | Cool < 4oC | 7 days | |||
| S | 8oz | G | Cool < 4oC | 14 days | |||
| SW | 8oz | G | Cool < 4oC | 14 days | |||
| TCLP | 16oz | G | Cool < 4oC | 14 days |
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GC ANALYSIS |
PARAMETER |
METHOD |
METHOD |
MATRIX |
VOLUME REQUIRED |
CONTAINER |
PRESERVATIVE |
HOLDING |
|
PCB's |
SW846
8082 OR EPA 608 |
Gas Chromatograph/ECD |
W |
2x1000 ml |
(Amber)G |
Cool < 4oC |
7 days |
| WW | 2x1000 ml | (Amber)G | Cool < 4oC | 7 days | |||
| S | 8oz | G | Cool < 4oC | 14 days | |||
| SW | 8oz | G | Cool < 4oC | 14 days | |||
| TCLP | 16oz | G | Cool < 4oC | 14 days | |||
| OIL | 25ml | G,P | Cool < 4oC | 14 days |
PARAMETER |
METHOD |
METHOD |
MATRIX |
VOLUME REQUIRED |
CONTAINER |
PRESERVATIVE |
HOLDING |
|
Pesticides |
SW846
8081 OR EPA 608 |
Gas Chromatograph/ECD |
W |
2x1000 ml |
(Amber)G |
Cool < 4oC |
7 days |
| WW | 2x1000 ml | (Amber)G | Cool < 4oC | 7 days | |||
| S | 8oz | G | Cool < 4oC | 14 days | |||
| SW | 8oz | G | Cool < 4oC | 14 days | |||
| TCLP | 16oz | G | Cool < 4oC | 14 days |
PARAMETER |
METHOD |
METHOD |
MATRIX |
VOLUME REQUIRED |
CONTAINER |
PRESERVATIVE |
HOLDING |
|
Total Petroleum Hydrocarbons (Diesel Range) |
SW 846 8015B(M)
|
Gas Chromatograph/ECD |
W |
2x1000 ml |
(Amber)G |
Cool < 4oC |
7 days |
| WW | 2x1000 ml | (Amber)G | Cool < 4oC | 7 days | |||
| S | 8oz | G | Cool < 4oC | 14 days | |||
| SW | 8oz | G | Cool < 4oC | 14 days | |||
| TCLP | 16oz | G | Cool < 4oC | 14 days |
PARAMETER |
METHOD |
METHOD |
MATRIX |
VOLUME REQUIRED |
CONTAINER |
PRESERVATIVE |
HOLDING |
|
Total Petroleum Hydrocarbons (Gasoline Range) |
SW 846 8015B(M)
|
Gas Chromatograph/ECD |
W |
3x40 ml |
G* |
Cool < 4oC |
14 days |
| WW | 3x40 ml | G* | Cool < 4oC | 14 days | |||
| S | 4oz | G | Cool < 4oC | 14 days | |||
| SW | 4oz | G | Cool < 4oC | 14 days | |||
| TCLP | 8oz | G | Cool < 4oC | 14 days |
|
40 ml zero headspace vial required Volatile Organic Compounds |
| SW 846 8260 |
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Dichlorodifluoromethane Chloromethane Vinyl chloride Bromomethane Chloroethane Trichlorofluoromethane Diethyl ether Acetone 1,1-Dichloroethene Methylene chloride trans-1,2-Dichloroethene 1,1-Dichloroethane 2-Butanone (MEK) 2,2-Dichloropropane cis-1,2-Dichloroethene Ethyl acetate Chloroform Bromochloromethane 1,1,1-Trichloroethane 1,1-Dichloropropene Carbon tetrachloride 1,2-Dichloroethane Benzene 2-Pentanone Trichloroethene 1,2-Dichloropropane Bromodichloromethane Dibromomethane |
4-Methyl-2-pentanone (MIBK) 4-Isopropyltoluene cis-1,3-Dichloropropene 1,3-Dichlorobenzene Toluene 1,4-Dichlorobenzene trans-1,3-Dichloropropene n-Butylbenzene 1,1,2-Trichloroethane 1,2-Dichlorobenzene 2-Hexanone 1,2-Dibromo-3-chloropropane 1,3-Dichloropropane 1,2,4-Trichlorobenzene Tetrachloroethene Hexachlorobutadiene Dibromochloromethane Naphthalene 1,2-Dibromoethane (EDB) 1,2,3-Trichlorobenzene Chlorobenzene 1,1,1,2-Tetrachloroethane Ethylbenzene p&m-Xylene o-Xylene Styrene Bromoform Isopropylbenzene |
1,1,2,2-Tetrachloroethane 1,2,3-Trichloropropane n-Propylbenzene Bromobenzene 1,3,5-Trimethylbenzene 2-Chlorotoluene 4-Chlorotoluene tert-Butylbenzene 1,2,4-Trimethylbenzene sec-Butylbenzene |
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Volatile Organic Compounds |
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Priority Pollutants |
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Dichlorodifluoromethane Vinyl chloride Bromomethane Chloroethane Trichlorofluoromethane 1,1-Dichloroethene Methylene chloride trans-1,2-Dichloroethene 1,1-Dichloroethane Chloroform 2-chloroethylvinyl ether 1,1,1-Trichloroethane Carbon tetrachloride 1,2-Dichloroethane Benzene |
cis-1,3-Dichloropropene Toluene trans-1,3-Dichloropropene 1,1,2-Trichloroethane Tetrachloroethene Dibromochloromethane Chlorobenzene Ethylbenzene Bromoform 1,1,2,2-Tetrachloroethane 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,2-Dichlorobenzene Methyl Bromide Methyl Chloride |
Acrolein Acryonitrile Trichloroethene 1,2-Dichloropropane Bromodichloromethane |
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TTO |
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Vinyl chloride Chloroethane 1,1-Dichloroethene Methylene chloride trans-1,2-Dichloroethene 1,1-Dichloroethane Chloroform 2-chloroethylvinyl ether 1,1,1-Trichloroethane Carbon tetrachloride 1,2-Dichloroethane Benzene |
cis-1,3-Dichloropropene Toluene trans-1,3-Dichloropropene 1,1,2-Trichloroethane Tetrachloroethene Dibromochloromethane Chlorobenzene Ethylbenzene Bromoform 1,1,2,2-Tetrachloroethane Methyl Bromide Methyl Chloride |
Acrolein Acryonitrile Trichloroethene 1,2-Dichloropropane Bromodichloromethane |
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| Target Compound List (TCL) |
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Vinyl acetate Vinyl chloride Acetone Chloroethane Carbon disulfide 1,1-Dichloroethene Methylene chloride 2-Butanone (MEK) 1,1-Dichloroethane Chloroform 2-Hexanone 1,1,1-Trichloroethane Carbon tetrachloride 1,2-Dichloroethane Benzene cis-1,2-Dichloroethene trans-1,2-Dichloroethene Trichloroethene 1,2-Dichloropropane Bromodichloromethane
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cis-1,3-Dichloropropene Toluene trans-1,3-Dichloropropene 1,1,2-Trichloroethane Tetrachloroethene Dibromochloromethane Chlorobenzene Ethylbenzene Bromoform 1,1,2,2-Tetrachloroethane Styrene 4-Methyl-2-pentanone (MIBK) Xylenes (Total) Methyl Bromide Methyl Chloride |
Acrolein Acryonitrile Trichloroethene 1,2-Dichloropropane Bromodichloromethane |
| Toxic Chemical Leaching Procedure (TCLP) |
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Vinyl chloride 1,1-Dichloroethene 2-Butanone (MEK) Chloroform Carbon tetrachloride 1,2-Dichloroethane Benzene Trichloroethene |
Tetrachloroethene Chlorobenzene 1,4-Dichlorobenzene |
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Semi-Volatile Organic Compounds |
|
8270C |
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N-nitrosodimethylamine Pyridine Phenol bis (2-Chloroethyl) ether 2-Chlorophenol 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,2-Dichlorobenzene 2-Methylphenol 4-Methylphenol n-Nitroso-di-n-propylamine Hexachloroethane Nitrobenzene Isophorone 2-Nitrophenol 2,4-Dimethylphenol Benzoic Acid bis (2-chloroethoxy) methane 2,4-Dichlorophenol 1,2,4-Trichlorobenzene Naphthalene 4-Chloroaniline Hexachlorobutadiene 4-Chloro-3-methylphenol
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2-Methylnaphthalene Hexachlorocyclopentadiene 2,4,6-Trichlorophenol 2,4,5-Trichlorophenol 2-Chloronaphthalene 2-Nitroaniline Dimethylphathalate Acenaphthylene 3-Nitroaniline Acenaphthene 2,4-Dinitrophenol 4-Nitrophenol Dibenzofuran 2,4-Dinitrotoluene 2,6-Dinitrotoluene Diethylphthalate 4-Chlorophenyl phenyl ether Fluorene 4-Nitroaniline 4,6-Dinitro-2-methylphenol 4-Bromophenyl phenyl ether Hexachlorobenzene Pentachlorophenol Phenanthrene |
Anthracene Carbazole Di-n-butylphthalate Fluoranthene Benzidine Pyrene Butylbenzylphthalate 3,3'-Dichlorobenzidine Benzo (a) anthracene bis (2-Ethylhexyl) phthalate Chrysene Di-n-octyl phthalate Benzo (b) fluoranthene Benzo (k) fluroanthene Benzo (a) pyrene Indeno (1,2,3-cd) pyrene Dibenz(a,h) anthracene Benzo (g,h,i) perylene Azobenzene bis (2-chloroisopropyl) ether |
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Semi-Volatile Organic Compounds |
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Priority Pollutants |
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N-nitrosodimethylamine Phenol bis (2-Chloroethyl) ether 2-Chlorophenol Hexachloroethane Nitrobenzene Isophorone 2-Nitrophenol 2,4-Dimethylphenol bis (2-chloroethoxy) methane 2,4-Dichlorophenol 1,2,4-Trichlorobenzene Naphthalene Hexachlorobutadiene 4-Chloro-3-methylphenol 1,2-Diphenylhydrazine |
Hexachlorocyclopentadiene 2,4,6-Trichlorophenol 2-Chloronaphthalene Dimethylphathalate Acenaphthylene Acenaphthene 2,4-Dinitrophenol 4-Nitrophenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene Diethylphthalate 4-Chlorophenyl phenyl ether Fluorene 4,6-Dinitro-2-methylphenol 4-Bromophenyl phenyl ether Hexachlorobenzene Pentachlorophenol Phenanthrene |
Anthracene Di-n-butylphthalate Fluoranthene Benzidine Pyrene Butylbenzylphthalate 3,3'-Dichlorobenzidine Benzo (a) anthracene bis (2-Ethylhexyl) phthalate Chrysene Di-n-octyl phthalate Benzo (b) fluoranthene Benzo (k) fluroanthene Benzo (a) pyrene Indeno (1,2,3-cd) pyrene Dibenz(a,h) anthracene Benzo (g,h,i) perylene bis (2-chloroisopropyl) ether |
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TTO |
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Phenol bis (2-Chloroethyl) ether 2-Chlorophenol 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,2-Dichlorobenzene n-Nitroso-di-n-propylamine Hexachloroethane Nitrobenzene Isophorone 2-Nitrophenol 2,4-Dimethylphenol bis (2-chloroethoxy) methane 2,4-Dichlorophenol 1,2,4-Trichlorobenzene Naphthalene Hexachlorobutadiene 4-Chloro-3-methylphenol 1,2-Diphenylhydrazine
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Hexachlorocyclopentadiene 2,4,6-Trichlorophenol 2-Chloronaphthalene Dimethylphathalate Acenaphthylene Acenaphthene 2,4-Dinitrophenol 4-Nitrophenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene Diethylphthalate 4-Chlorophenyl phenyl ether Fluorene 4,6-Dinitro-2-methylphenol 4-Bromophenyl phenyl ether Hexachlorobenzene Pentachlorophenol Phenanthrene Diphenylamine |
Anthracene Di-n-butylphthalate Fluoranthene Benzidine Pyrene Butylbenzylphthalate 3,3'-Dichlorobenzidine Benzo (a) anthracene bis (2-Ethylhexyl) phthalate Chrysene Di-n-octyl phthalate Benzo (b) fluoranthene Benzo (k) fluroanthene Benzo (a) pyrene Indeno (1,2,3-cd) pyrene Dibenz(a,h) anthracene Benzo (g,h,i) perylene bis (2-chloroisopropyl) ether |
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Semi-Volatile Organic Compounds |
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Target Compound List (TCL) |
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Phenol bis (2-Chloroethyl) ether 2-Chlorophenol 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,2-Dichlorobenzene 2-Methylphenol 3,4-Methylphenol n-Nitroso-di-n-propylamine Hexachloroethane Nitrobenzene Isophorone 2-Nitrophenol 2,4-Dimethylphenol bis (2-chloroethoxy) methane 2,4-Dichlorophenol 1,2,4-Trichlorobenzene Naphthalene 4-Chloroaniline Hexachlorobutadiene 4-Chloro-3-methylphenol 1,1’-Biphenyl Acetophenone Atrazine |
2-Methylnaphthalene Hexachlorocyclopentadiene 2,4,6-Trichlorophenol 2,4,5-Trichlorophenol 2-Chloronaphthalene 2-Nitroaniline Dimethylphathalate Acenaphthylene 3-Nitroaniline Acenaphthene 2,4-Dinitrophenol 4-Nitrophenol Dibenzofuran 2,4-Dinitrotoluene 2,6-Dinitrotoluene Diethylphthalate 4-Chlorophenyl phenyl ether Fluorene 4-Nitroaniline 4,6-Dinitro-2-methylphenol 4-Bromophenyl phenyl ether Hexachlorobenzene Pentachlorophenol Phenanthrene |
Anthracene Carbazole Di-n-butylphthalate Fluoranthene Benzidine Pyrene Butylbenzylphthalate 3,3'-Dichlorobenzidine Benzo (a) anthracene bis (2-Ethylhexyl) phthalate Chrysene Di-n-octyl phthalate Benzo (b) fluoranthene Benzo (k) fluroanthene Benzo (a) pyrene Indeno (1,2,3-cd) pyrene Dibenz(a,h) anthracene Benzo (g,h,i) perylene bis (2-chloroisopropyl) ether Benzaldehyde Caprolactam Diphenylamine |
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Toxic Chemical Leaching Procedure (TCLP) |
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Pyridine 1,4-Dichlorobenzene 2-Methylphenol 3,4-Methylphenol Hexachloroethane Nitrobenzene Hexachlorobutadiene |
2,4,6-Trichlorophenol 2,4,5-Trichlorophenol 2,4-Dinitrotoluene Hexachlorobenzene Pentachlorophenol
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Toxic Chemical Leaching Procedure (TCLP) |
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Pyridine 1,4-Dichlorobenzene 2-Methylphenol 3,4-Methylphenol Hexachloroethane Nitrobenzene Hexachlorobutadiene |
2,4,6-Trichlorophenol 2,4,5-Trichlorophenol 2,4-Dinitrotoluene Hexachlorobenzene Pentachlorophenol
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Pesticide/PCB/Herbicide Compounds |
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Pesticides SW 846 8081 |
PCB's SW846 8082 |
Herbicides SW 846 8151 |
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Aldrin Alpha-BHC Beta-BHC Delta-BHC Gamma BHC (Lindane) Chlordane Alpha-Chlordane Gamma-Chlordane 4,4’-DDD 4,4’-DDE 4,4’ DDT Dieldrin Endosulfan I Endosulfan II Endosulfan Sulfate Endrin Endrin Aldehyde Endrin Ketone Heptachlor Heptachlor Epoxide Methoxychlor Toxaphene |
PCB-1016 PCB-1221 PCB-1232 PCB-1242 PCB-1248 PCB-1254 PCB-1260
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2,4-D 2,4 –DB Dicamba Dichlorprop MCPA MCPP 2,4,5-TP (Silvex) 2,4,5-T
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Pesticides Priority Pollutants |
PCB’s Priority Pollutants |
Herbicides Priority Pollutants |
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Alpha-BHC Beta-BHC Delta-BHC Gamma BHC (Lindane) 4,4’-DDD 4,4’-DDE 4,4’ DDT Dieldrin Endosulfan I Endosulfan II Endosulfan Sulfate Endrin Endrin Aldehyde Heptachlor Heptachlor Epoxide Methoxychlor Toxaphene |
PCB-1016 PCB-1221 PCB-1232 PCB-1242 PCB-1248 PCB-1254 PCB-1260
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Pesticides Target Compound List (TCL) |
PCB's Target Compound List (TCL) |
Herbicides Target Compound List (TCL) |
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Aldrin Alpha-BHC Beta-BHC Delta-BHC Gamma BHC (Lindane) Alpha-Chlordane Gamma-Chlordane 4,4’-DDD 4,4’-DDE 4,4’ DDT Dieldrin Endosulfan I Endosulfan II Endosulfan Sulfate Endrin Endrin Ketone Heptachlor Heptachlor Epoxide Methoxychlor Toxaphene |
PCB-1016 PCB-1221 PCB-1232 PCB-1242 PCB-1248 PCB-1254 PCB-1260
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Pesticides TCLP |
PCB's TCLP |
Herbicides TCLP |
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Gamma BHC (Lindane) Endrin Heptachlor Heptachlor Epoxide Methoxychlor Toxaphene Chlordane |
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2,4-D 2,4,5-TP (Silvex) |
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Pesticides TTO |
PCB's TTO | |
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Aldrin Alpha-BHC Beta-BHC Delta-BHC Gamma BHC (Lindane) 4,4’-DDD 4,4’-DDE 4,4’ DDT Dieldrin |
Endosulfan I Endosulfan II Endosulfan Sulfate Endrin Endrin Aldehyde Heptachlor Heptachlor Epoxide Toxaphene |
PCB-1016 PCB-1221 PCB-1232 PCB-1242 PCB-1248 PCB-1254 PCB-1260
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