Inorganic Ananlysis

Inorganic Analysis

PARAMETER	METHOD	METHOD DESCRIPTION	MATRIX	VOLUME REQUIRED	CONTAINER	PRESERVATIVE	HOLDING TIME
Titrametric	SM2310B OR EPA 305.1	Acidity	W	1000 ml	P,G	Cool < 4^oC
Titrametric	SM2310B OR EPA 305.1	Acidity	WW	1000 ml	P,G	Cool < 4^oC
Alkalinity, Total (as CaCO₃)	EPA 310.1	Titrametric	W	1000 ml	P,G	Cool < 4^oC	14 days
Alkalinity, Total (as CaCO₃)	EPA 310.1	Titrametric	WW	1000 ml	P,G	Cool < 4^oC	14 days
Bicarbonates(as CaCO₃)	EPA 310.1	Titrametric	W	1000 ml	P,G	Cool < 4^oC	14 days
Bicarbonates(as CaCO₃)	EPA 310.1	Titrametric	WW	1000 ml	P,G	Cool < 4^oC	14 days
Biological Oxygen Demand (5 Day)	SM5210	Electrode	W	1000 ml	P,G	Cool < 4^oC	48 hours
Biological Oxygen Demand (5 Day)	SM5210	Electrode	WW	1000 ml	P,G	Cool < 4^oC	48 hours
Biological Oxygen Demand (5 Day) Carbonaceous	SM5210	Electrode	W	1000 ml	P,G	Cool < 4^oC	48 hours
Biological Oxygen Demand (5 Day) Carbonaceous	SM5210	Electrode	WW	1000 ml	P,G	Cool < 4^oC	48 hours
Carbon (Dissolved)	EPA 415.2	UV promuted, persulfate oxidation	W	200 ml	P,G	Cool < 4^oC	14 days
Carbon (Dissolved)	EPA 415.2	UV promuted, persulfate oxidation	WW	200 ml	P,G	Cool < 4^oC	14 days
Carbon (Total)	EPA 415.2	UV promuted, persulfate oxidation	W	200 ml	P,G	Cool < 4^oC	14 days
Carbon (Total)	EPA 415.2	UV promuted, persulfate oxidation	WW	200 ml	P,G	Cool < 4^oC	14 days
Carbon (Total Inorganic)	EPA 415.2	UV promuted, persulfate oxidation	W	200 ml	P,G	Cool < 4^oC	14 days
Carbon (Total Inorganic)	EPA 415.2	UV promuted, persulfate oxidation	WW	200 ml	P,G	Cool < 4^oC	14 days
Carbon (Total Organic)	EPA 415.2	UV promuted, persulfate oxidation	W	200 ml	P,G	Cool < 4^oC H₂SO₄ to pH< 2	28 days
Carbon (Total Organic)	EPA 415.2	UV promuted, persulfate oxidation	WW	200 ml	P,G	Cool < 4^oC H₂SO₄ to pH< 2	28 days
Carbonates (as CaCo₃)	EPA 310.1	Titrametric	W	1000 ml	P,G	Cool < 4^oC	14 days
Carbonates (as CaCo₃)	EPA 310.1	Titrametric	WW	1000 ml	P,G	Cool < 4^oC	14 days
Chemical Oxygen Demand (COD)	HACH 8000/EPA 410.2	Colormetric	W	200 ml	P,G	Cool < 4^oC	48 hours
Chemical Oxygen Demand (COD)	HACH 8000/EPA 410.2	Colormetric	WW	200 ml	P,G	Cool < 4^oC	48 hours
Chlorine (Total Residual)	EPA 330.5	Colormetric	W	1000 ml	P,G	Cool < 4^oC	48 hours
Chlorine (Total Residual)	EPA 330.5	Colormetric	WW	1000 ml	P,G	Cool < 4^oC	48 hours
Chromium, Hexavalent	SW846 7196A Or SM3500-Cr D	Colormetric	W	1000 ml	P,G	Cool < 4^oC	24 hours
			WW	1000 ml	P,G	Cool < 4^oC	24 hours
			S	100 g	P,G	Cool < 4^oC	NA
			SW	100 g	P,G	Cool < 4^oC	NA
Conductivity, Specific	EPA 120.1	Electrode	W	1000 ml	P,G	Cool < 4^oC	48 hours
Conductivity, Specific	EPA 120.1	Electrode	WW	1000 ml	P,G	Cool < 4^oC	48 hours

PARAMETER	METHOD	METHOD DESCRIPTION	MATRIX	VOLUME REQUIRED	CONTAINER	PRESERVATIVE	HOLDING TIME
Corrosivity	SW 846 9040A or SW 846 9045B	Electrode	W	1000 ml	P,G	Cool < 4^oC	NA
			WW	1000 ml	P,G	Cool < 4^oC	NA
			S	50g	P,G	Cool < 4^oC	NA
			SW	50g	P,G	Cool < 4^oC	NA
Cyanide (Amenable)	EPA 332.1,335.2 Or SW846 9010,9014	Colormetric	W	2000 ml	P,G	Cool < 4^oC NaOH to pH >12	14 days
			WW	2000 ml	P,G	Cool < 4^oC NaOH to pH >12	14 days
			S	100g	P,G	Cool < 4^oC	14 days
			SW	100g	P,G	Cool < 4^oC	14 days
Cyanide (Reactive)	EPA 332.1,335.2 Or SW846 9010,9014	Colormetric	W	1000 ml	P,G	Cool < 4^oC	NA
			WW	1000 ml	P,G	Cool < 4^oC	NA
			S	50g	P,G	Cool < 4^oC	NA
			SW	50g	P,G	Cool < 4^oC	NA
Cyanide (Total)	EPA 332.1,335.2 Or SW846 9010,9014	Colormetric	W	1000 ml	P,G	Cool < 4^oC	48 hours
			WW	1000 ml	P,G	Cool < 4^oC	48 hours
					P,G
					P,G
Flash Point (Ignitability)	SW846 1010	Closed-cup	W	1000 ml	P,G	Cool < 4^oC	48 hours
			WW	1000 ml	P,G	Cool < 4^oC	48 hours
			S	150g	P,G
			SW	150g	P,G
Fluoride	EPA 340.2	Electrode	W	1000 ml	P,G	Cool < 4^oC	28 days
Fluoride	EPA 340.2	Electrode	WW	1000 ml	P,G	Cool < 4^oC	28 days
Hardness (Total)	EPA 130.2	Titrametric	W	1000 ml	P,G	HNO₃ to pH< 2	14 days
Hardness (Total)	EPA 130.2	Titrametric	WW	1000 ml	P,G	HNO₃ to pH< 2	14 days
Moisture (LOD)	ASTM D2216-92	Gravimetric	W	1000 ml	P,G	Cool < 4^oC	NA
			WW	1000 ml	P,G	Cool < 4^oC	NA
			S	50g	P,G	Cool < 4^oC	NA
			SW	50g	P,G	Cool < 4^oC	NA
Nitrogen (N) , Ammonia	EPA 350.3	Electrode	W	250 ml	P,G	Cool < 4^oC H₂SO₄ to pH< 2	28 days
Nitrogen (N) , Ammonia	EPA 350.3	Electrode	WW	250 ml	P,G	Cool < 4^oC H₂SO₄ to pH< 2	28 days
Nitrogen (N), Kjeldahl (TKN)	EPA 351.3	Titrametric	W	1000 ml	P,G	Cool < 4^oC H₂SO₄ to pH< 2	14 days
Nitrogen (N), Kjeldahl (TKN)	EPA 351.3	Titrametric	WW	1000 ml	P,G	Cool < 4^oC H₂SO₄ to pH< 2	14 days

PARAMETER	METHOD	METHOD DESCRIPTION	MATRIX	VOLUME REQUIRED	CONTAINER	PRESERVATIVE	HOLDING TIME
Nitrogen (N), Nitrate	EPA 352.1 Or SM 4500-NO3 D	Colormetric Or Electrode	W	200 ml	P,G	Cool < 4^oC H₂SO₄ to pH< 2	14 days
Nitrogen (N), Nitrate	EPA 352.1 Or SM 4500-NO3 D	Colormetric Or Electrode	WW	200 ml	P,G	Cool < 4^oC H₂SO₄ to pH< 2	14 days
Nitrogen (N), Nitrite	EPA 354.1	Colormetric	W	500 ml	P,G	Cool < 4^oC H₂SO₄ to pH< 2	14 days
Nitrogen (N), Nitrite	EPA 354.1	Colormetric	WW	500 ml	P,G	Cool < 4^oC H₂SO₄ to pH< 2	14 days
Oil & Grease	EPA 1664	Gravimetric	W	1000 ml	G(Amber)	Cool < 4^oC H₂SO₄ to pH< 2	28 days
Oil & Grease	EPA 1664	Gravimetric	WW	1000 ml	G(Amber)	Cool < 4^oC H₂SO₄ to pH< 2	28 days
Oxygen, Dissolved	SM5210	Electrode	W	1000 ml	P,G	Cool < 4^oC	48 hours
			WW	1000 ml	P,G	Cool < 4^oC	48 hours
					P,G
					P,G
Paint Filter Test	SW846 9095A	Filter	W	1000 ml	P,G	Cool < 4^oC	NA
			WW	1000 ml	P,G	Cool < 4^oC	NA
			S	150g	P,G	Cool < 4^oC	NA
			SW	150g	P,G	Cool < 4^oC	NA
pH	EPA150.1 or SW 846 9040A	Electrode	W	100 ml	P,G	Cool < 4^oC	ASAP
			WW	100ml	P,G	Cool < 4^oC	ASAP
			S	50g	P,G	Cool < 4^oC	ASAP
			SW	50g	P,G	Cool < 4^oC	ASAP
Phenols , Total	EPA 420.1 Or SW 846 9065	Colormetric	W	1000 ml	P,G	Cool < 4^oC H₂SO₄ to pH< 2	28 days
Phenols , Total	EPA 420.1 Or SW 846 9065	Colormetric	WW	1000 ml	P,G	Cool < 4^oC H₂SO₄ to pH< 2	28 days
Phosphorus, Ortho	SM 4500P D	Colormetric	W	1000 ml	P,G	Cool < 4^oC	48 hours
Phosphorus, Ortho	SM 4500P D	Colormetric	WW	1000 ml	P,G	Cool < 4^oC	48 hours
Phosphorus, Total	SM 4500P D	Colormetric	W	1000 ml	P,G	Cool < 4^oC	14 days
Phosphorus, Total	SM 4500P D	Colormetric	WW	1000 ml	P,G	Cool < 4^oC	14 days
Phosphate Total	SM 4500P D	Colormetric	W	1000 ml	P,G	Cool < 4^oC H₂SO₄ to pH< 2	14 days
Phosphate Total	SM 4500P D	Colormetric	WW	1000 ml	P,G	Cool < 4^oC H₂SO₄ to pH< 2	14 days
Solids, Total Dissolved (TDS)	EPA 160.1	Gravimetric	W	1000 ml	P	Cool < 4^oC	7 days
Solids, Total Dissolved (TDS)	EPA 160.1	Gravimetric	WW	1000 ml	P	Cool < 4^oC	7 days
Solids, Total Suspended (TSS)	EPA 160.2	Gravimetric	W	1000 ml	P	Cool < 4^oC	7 days
Solids, Total Suspended (TSS)	EPA 160.2	Gravimetric	WW	1000 ml	P	Cool < 4^oC	7 days

PARAMETER	METHOD	METHOD DESCRIPTION	MATRIX	VOLUME REQUIRED	CONTAINER	PRESERVATIVE	HOLDING TIME
Solids, Total	EPA 160.3	Gravimetric	W	1000 ml	P	Cool < 4^oC	7 days
Solids, Total	EPA 160.3	Gravimetric	WW	1000 ml	P	Cool < 4^oC	7 days
Sulfate	EPA 375.4	Colormetric or Turbimetric	W	1000 ml	P,G	Cool < 4^oC	28 days
Sulfate	EPA 375.4	Colormetric or Turbimetric	WW	1000 ml	P,G	Cool < 4^oC	28 days
Sulfide , Reactive	SW 846 7.3.4 Or EPA 376.1	Titrametric	W	1000 ml	P,G	Cool < 4^oC	NA
			WW	1000 ml	P,G	Cool < 4^oC	NA
			S	50g	P,G	Cool < 4^oC	NA
			SW	50g	P,G	Cool < 4^oC	NA
Sulfide , Total	EPA 376.1	Titrametric	W	100 ml	P,G	Cool < 4^oC NaOH to pH >12	7 days
			WW	100 ml	P,G	Cool < 4^oC NaOH to pH >12	7 days
			S	50g	P,G	Cool < 4^oC	NA
			SW	50g	P,G	Cool < 4^oC	NA
Total Organic Halides (TOX)	SW846 9020B	Coulumetric	W	1000 ml	G(Amber)	Cool < 4^oC HNO₃ to pH< 2	28 days
			WW	1000 ml	G(Amber)	Cool < 4^oC HNO₃ to pH< 2	28 days
			S	50g	P,G	Cool < 4^oC	28 days
			SW	50g	P,G	Cool < 4^oC	28 days
Turbidity	EPA 180.1	Nephelumetric	W	500 ml	P,G	Cool < 4^oC	48 days
Turbidity	EPA 180.1	Nephelumetric	WW	500 ml	P,G	Cool < 4^oC	48 days

PARAMETER

Electrode

Electrode

PARAMETER

Colormetric

Closed-cup

PARAMETER

Colormetric Or Electrode

Electrode

Filter

PARAMETER

Gravimetric

Colormetric or Turbimetric

Colormetric
Or
Electrode

Colormetric
or
Turbimetric